Table 1
Summary of experimental data and measurement protocols.
| Data type | Measurement technique | Instrumentation/equipment | Spatial/temporal resolution | Sample size / data volume | Purpose/usage |
|---|---|---|---|---|---|
| Microstructure | X-ray micro-CT + Optical Microscopy | Micro-CT scanner (voxel size 5 μm), optical microscope | 3D volumes (voxel 5 μm resolution) | >1,000 microstructural volumes | Fiber volume fraction, porosity mapping for multiscale modeling input |
| Cure Kinetics | Differential Scanning Calorimetry (DSC) | TA Instruments DSC Q2000 | Time-resolved, seconds to minutes | >500 time points per specimen | Calibrate Arrhenius cure model parameters |
| Temperature Fields | Embedded Micro-Thermocouples + IR Thermography | Micro-thermocouples; FLIR infrared camera | Depth-resolved thermocouples; sub-second IR imaging | Distributed sensor network, continuous recording during curing | Capture spatial and temporal thermal gradients |
| Residual Stress | Embedded Strain Gauges | Vishay strain gauges calibrated per ASTM E251 | Local point measurements, ±2% accuracy | Minimum 5 specimens per configuration | Validate chemo-thermo-mechanical residual stress predictions |
| Mechanical Properties | Tensile and Flexural Testing | Universal testing machine (Instron) | Controlled strain rates, standard protocols ASTM D3039, D7264 | ≥5 specimens per |
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